Synthesis and Study of Potassium Hexabromoiridate(IV) |
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| Authors: | Gubanov A. I. Gromilov S. A. Korenev S. V. Venediktov A. B. Asanov I. P. |
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| Affiliation: | (1) Siberian Division, Russian Academy of Sciences, Institute of Inorganic Chemistry, pr. Akademika Lavrenteva 3, Novosibirsk, 6300900, Russia |
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| Abstract: | A new method of synthesis of potassium hexabromoiridate(IV) was developed. This complex was studied using X-ray diffraction and elemental analyses and electronic absoprtion, IR, and Raman spectroscopy methods. Crystallographic parameters: a = 10.298(5) Å, V = 1092.1 Å3, Z = 4, space group Fm3m,  (calcd) = 4.560 g/cm3; K2[PtCl6] structural type. The thermal decomposition of this salt in an inert atmosphere was investigated. |
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