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Microflow photochemistry—a reactor comparison study using the photochemical synthesis of terebic acid as a model reaction
Authors:Shin AidaKimitada Terao  Yasuhiro NishiyamaKiyomi Kakiuchi  Michael Oelgemöller
Institution:a Graduate School of Materials Science, Nara Institute of Science and Technology (NAIST), 8916-5 Takayama-cho, Ikoma, Nara 630-0101, Japan
b James Cook University, School of Pharmacy and Molecular Sciences, Center for Biodiscovery and Molecular Development of Therapeutics (BMDT), Townsville, QLD 4811, Australia
Abstract:The continuous-microflow photochemical synthesis of terebic acid from maleic acid was investigated in two different microreactor set-ups. The results were subsequently compared to analogue experiments in a conventional chamber reactor. Based on conversion rates, reactor design and energy efficiency calculations, the simple microcapillary reactor showed the best overall performance.
Keywords:Photochemistry  Microflow  Terebic acid  Photoaddition
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