Structure elucidation of casbane diterpenes from Croton argyrophyllus |
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Authors: | e Silva-Filho Francisco Artur Braz-Filho Raimundo Silveira Edilberto Rocha Lima Mary Anne Sousa |
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Affiliation: | Departamento de Química Organica e Inorganica, Centro de Ciências, Universidade Federal do Ceará, CP 12.200, 60.021-970, Fortaleza, CE, Brazil. |
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Abstract: | Two novel casbane diterpenes 1-hydroxy-(2E,6Z,12E)-casba-2,6,12-triene-4,5-dione (1) and 6E,12E-casba-1,3,6,12-tetraen-1,4-epoxy-5-one (2) were isolated from the ethanol extract of the stems of Croton argyrophyllus. Structural characterization including the relative stereochemistry of all compounds was established on the basis of spectroscopic methods, mainly 1D and 2D NMR, and HRESIMS. |
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Keywords: | NMR 1H NMR 13C NMR Croton argyrophyllus casbane diterpenes structure assignment |
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