Modification of Synthesis of 3-Chloro-4-(dichloromethyl)-5-hydroxy-2(5H)-furanone(MX) |
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| Authors: | Zhang Jinqu Zhu Zhen Zou Huixian Yang Minmin |
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| Institution: | 1. Department of Chemistry , Nanjing University , Nanjing, 210093, P.R., China;2. Department of Environmental Science and Engineering , Nanjing University , Nanjing, 210093, P.R., China |
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| Abstract: | Addition of chlorine to methyl 3-(dichloromethyl)-4,4-dichlorocrotonate (1), a critical procedure in the total synthesis of the title compound MX, was modified by using novel catalysts. A minor modification in the purification of MX was also described. |
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