Synthesis of Diacetals of 2,2-bis(Hydroxymethyl)-1,3-Propanediol Under Microwave Irradiation |
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| Authors: | Cun-De Wang Xin-Zhong Shi Ren-Jian Xie |
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| Institution: | 1. Department of Chemistry , Institute of Technology, Yangzhou University , Yangzhou, 225009, P. R. China;2. Department of Organic Chemistry , China Pharmaceutical University , Nanjing, 210009, P. R. China |
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| Abstract: | Nine diacetals (3a-i) of 2,2-bis(hydroxymethyl)-1,3-propanediol (2) were prepared by condensation of aldehydes with 2 under microwave irradiation in the presence of TsOH without solvent. |
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