A Short,Efficient, Multigram Synthetic Route to 2,3-Dimethylfuran and Some of its 2-Substituted Derivatives |
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| Authors: | Daniel Végh Peter Zalupsky Jaroslav Kováč |
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| Institution: | Department of Organic Chemistry , Slovak Technical University , CS-812 37, Bratislava, Czechoslovakia |
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| Abstract: | A laboratory, multigram (1000 g in an hour) preparation procedure for 2,3-dimethylfuran, based on the frequently repeated thermal cyclization of (Z) 3-methyl-2-penten-4-yn-1-ol, as well as its subsequent formylation, acetylation and oxidation is described. |
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