Organic Chemistry Without Solvent. Improvements to the One Step Preparation of Dibenzyl Sulphones |
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| Authors: | By André Loupy Jean Sansoulet Alan R. Harris |
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| Affiliation: | 1. Laboratoire des Reactions Selectives sur Supports , ICMO, UA478 du CNRS - Universite Paris Sud , Batiment 410, 91405, Orsay, France;2. Chemical Process R &3. D Dept. , Fisons PLC, Pharmaceutical Division, R&4. D Labs. , Bakewell Rd, Loughborough, LEll ORH, Leics, England |
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| Abstract: | Dibenzyl sulphones can be prepared from the corresponding benzyl halide under mild, economic and efficient conditions, using either sodium dithionite / Aliquat, or sodium formaldehyde sulphoxylate /potassium carbonate in the absence of solvent. |
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