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A Convenient Method for the Synthesis of bis-Trifluoroethyl Phosphonoacetates |
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| Authors: | Carl Patois Philippe Savignac Elie About-Jaudet Noël Collignon |
| Institution: | 1. Laboratoire de Chimie du Phosphore et des Métaux de Transition , DCPH , Ecole Polytechnique, 91128, Palaiseau, Cedex, FRANCE;2. Laboratoire des Composés Organophosphorés INSA-IRCOF , BP 08, 76131, Mont-Saint-Aignan, Cedex, FRANCE |
| Abstract: | bis-Trifluoroethyl phosphonoacetates were easily obtained by condensation of bis-trifluoroethyl alkylphosphonates with alkyl chloroformates in the presence of 2 equivalents of lithium hexamethyldisilazane (LiHMDS). |
| Keywords: | |