| (E)-3-(4一羟苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物核磁共振特征与构象分析 |
| |
| 引用本文： | 朱传钧,朱美玲,崔育新,姜标,郑锦鸿. (E)-3-(4一羟苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物核磁共振特征与构象分析[J]. 波谱学杂志, 2011, 28(3): 390-398 |
| |
| 作者姓名： | 朱传钧 朱美玲 崔育新 姜标 郑锦鸿 |
| |
| 作者单位： | 中国科学院上海有机化学研究所,上海 200032;上海精细化工火炬创新创业园分析中心,上海 201512;汕头大学医学院,广东汕头,515031;天然药物及仿生药物国家重点实验室(北京大学),北京,100191;中国科学院上海有机化学研究所,上海,200032 |
| |
| 摘 要： | 设计并合成了一系列(E)-3-(4-羟苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物. 通过一维和二维核磁共振实验完成了1H和13C信号的指认. 通过ROESY、变温实验和分子模拟技术对这类化合物的构象进行了分析.
|
| 关 键 词： | 核磁共振 指认 二维核磁共振 (E)-3-(4-羟苯基)-1-(哌啶-1-基)丙-2-烯-1-酮衍生物 构象分析 |
| 收稿时间： | 2010-11-10 |
NMR Characteristics and Conformational Analysis of (E)-3-(4-hydroxyphenyl)-1-(piperidin-1-yl) prop-2-en-1-one Derivatives |
| |
| ZHU Chuan-jun,,ZHU Mei-ling,CUI Yu-xin,JIANG Biao,ZHENG Jin-hong,Beijing ,China). NMR Characteristics and Conformational Analysis of (E)-3-(4-hydroxyphenyl)-1-(piperidin-1-yl) prop-2-en-1-one Derivatives[J]. Chinese Journal of Magnetic Resonance, 2011, 28(3): 390-398 |
| |
| Authors: | ZHU Chuan-jun ZHU Mei-ling CUI Yu-xin JIANG Biao ZHENG Jin-hong Beijing China) |
| |
| Affiliation: | 1. Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China;;2. Shanghai Torch Innovation Park of Fine Chemical Industry Analysis Center, Shanghai 201512, China;;3. Medical College, Shantou University, Shantou 515031, China; ;4. State Key Laboratory of Natural and Biomimetic Drugs (Peking University), Beijing 100191, China |
| |
| Abstract: | A new series of(E)-3-(4-hydroxyphenyl)-1-(piperidin-1-yl)prop-2-en-1-one derivatives were designed and synthesized.1H and 13C NMR spectral assignments of these compounds were presented by one-and two-dimensional NMR experiments and conformations were analyzed by ROESY,variable-temperature NMR spectroscopy and molecular modeling. |
| |
| Keywords: | NMR assignment 2D NMR (E)-3-(4-hydroxyphenyl)-1-(piperidin-1-yl)prop-2-en-1-one derivatives conformational analysis |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《波谱学杂志》浏览原始摘要信息 |
|
点击此处可从《波谱学杂志》下载全文 |
|
