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共沉淀分离-ICP-MS快速测定卤水中稀土元素
引用本文:李吉生,郭爱武,邢谦,李邦民. 共沉淀分离-ICP-MS快速测定卤水中稀土元素[J]. 光谱实验室, 2009, 26(6): 1676-1678
作者姓名:李吉生  郭爱武  邢谦  李邦民
作者单位:青海省地质矿产测试应用中心,西宁市盐湖巷15号,810008 
摘    要:在卤水中加入适量的铁盐,以氨水为沉淀剂生成Fe(OH)3沉淀,稀土同时也被沉淀,分离、富集卤水中的稀土元素,用ICP-MS测定稀土元素,加标回收率在90.0%—110.0%,测定精密度RSD0.83%—3.21%,方法简单、快速、实用。

关 键 词:卤水  稀土元素  沉淀分离  富集  电感耦合等离子体-质谱

Separation and Determination of Rare Earth Element in the Halogenatehal Water by ICP-MS with Precipitation
LI Ji-Sheng GUO Ai-Wu XING Qian LI Bang-Min. Separation and Determination of Rare Earth Element in the Halogenatehal Water by ICP-MS with Precipitation[J]. Chinese Journal of Spectroscopy Laboratory, 2009, 26(6): 1676-1678
Authors:LI Ji-Sheng GUO Ai-Wu XING Qian LI Bang-Min
Affiliation:LI Ji-Sheng GUO Ai-Wu XING Qian LI Bang-Min (Qinghai Geology Mineral Testing Application Center,Xining 810008,P.R.China)
Abstract:The co-prepriates of iron salt in the halogenatehal water by the ammonia of Fe(OH)_3 and the rare earth clement, and measured by the ICP-MS. The standard recovery is in the range of 90.0%-110.0% with the RSD of 0. 83%-3.21%. The method is simple,quick and practicality.
Keywords:The Halogenatehal Water  Rare Earth Element  Precipitate to Separate  Enrich  ICP-MS
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