| Synthesis of Diphenyl α-（Dipropoxyphosphoramido）alkyl-phosphonates |
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| 引用本文： | 崔占伟 张建锋 苗志伟 陈茹玉. Synthesis of Diphenyl α-（Dipropoxyphosphoramido）alkyl-phosphonates[J]. 中国化学, 2007, 25(10): 1551-1554. DOI: 10.1002/cjoc.200790285 |
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| 作者姓名： | 崔占伟 张建锋 苗志伟 陈茹玉 |
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| 作者单位： | State Key Laboratory of Elemento-organic Chemistry, Research Institute of Elemento-organic Chemistry, Nankai University, Tianjin 300071, China |
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| 基金项目： | Project supported by the Committee of Science and Technology of Tianjin （No. 07JCZDJC04800） and Nankai University （No. J02044）. |
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| 摘 要： | A convenient method has been developed for the synthesis of diphenyl α-（dipropoxyphosphoramido）alkyl- phosphonates under mild conditions, namely the reaction of dipropyl phosphoramidate （1） with a para（un）substituted benzaldehyde or cyclicketone （2） and triphenyl phosphite （3） by a one-pot procedure with the aid of acetyl chloride.
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| 关 键 词： | 亚磷酸三苯酯 乙酰氯 α-氨基烷烃膦酸酯 合成 |
| 修稿时间： | 2007-02-27 |
Synthesis of Diphenyl α‐(Dipropoxyphosphoramido)alkylphosphonates |
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| CUI, Zhan-Wei ZHANG, Jian-Feng MIAO, Zhi-Wei CHEN, Ru-Yu. Synthesis of Diphenyl α‐(Dipropoxyphosphoramido)alkylphosphonates[J]. Chinese Journal of Chemistry, 2007, 25(10): 1551-1554. DOI: 10.1002/cjoc.200790285 |
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| Authors: | CUI Zhan-Wei ZHANG Jian-Feng MIAO Zhi-Wei CHEN Ru-Yu |
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| Affiliation: | State Key Laboratory of Elemento-organic Chemistry, Research Institute of Elemento-organic Chemistry, Nankai University, Tianjin 300071, China |
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| Abstract: | A convenient method has been developed for the synthesis of diphenyl α‐(dipropoxyphosphoramido)alkyl‐ phosphonates under mild conditions, namely the reaction of dipropyl phosphoramidate ( 1 ) with a para‐ (un)substituted benzaldehyde or cyclicketone ( 2 ) and triphenyl phosphite ( 3 ) by a one‐pot procedure with the aid of acetyl chloride. |
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| Keywords: | Mannich type reaction α‐aminoalkanephosphonate triphenyl phosphite acetyl chloride |
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