| A Practical Route to Synthesize 3,4-O-Isopropylidene-2- azidophytosphingosine from D-Galactose |
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| 引用本文： | 丁宁 刘运鹏 吕国凯 李英霞. A Practical Route to Synthesize 3,4-O-Isopropylidene-2- azidophytosphingosine from D-Galactose[J]. 中国化学, 2007, 25(8): 1069-1071. DOI: 10.1002/cjoc.200790197 |
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| 作者姓名： | 丁宁 刘运鹏 吕国凯 李英霞 |
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| 作者单位： | Key Laboratory of Marine Drug, The Ministry of Education of China, School of Medicine and Pharmacy, Ocean University of China, Qingdao, Shangdong 266003, China |
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| 基金项目： | Project supported by the National Basic Research Program of China （No. 2003CB716403）. |
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| 摘 要： | An efficient and practical route to synthesize （2S,3S,4R）-2-azido-3,4-O-isopropyllidene-1,3,4-octadecanetriol from D-galactose in 18% overall yield was described, which required ten steps of reactions and only four times column chromatography purification.
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| 关 键 词： | 醣脂 鞘糖脂 植物鞘氨醇 叠氮基植物鞘氨醇 合成 |
| 修稿时间： | 2007-02-092007-05-20 |
A Practical Route to Synthesize 3,4-O-Isopropylidene-2- azidophytosphingosine from D-Galactose |
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| DING Ning,LIU Yun-Peng,LU Guo-Kai, LI Ying-Xia. A Practical Route to Synthesize 3,4-O-Isopropylidene-2- azidophytosphingosine from D-Galactose[J]. Chinese Journal of Chemistry, 2007, 25(8): 1069-1071. DOI: 10.1002/cjoc.200790197 |
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| Authors: | DING Ning LIU Yun-Peng LU Guo-Kai LI Ying-Xia |
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| Affiliation: | Key Laboratory of Marine Drug, The Ministry of Education of China, School of Medicine and Pharmacy, Ocean University of China, Qingdao, Shangdong 266003, China |
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| Abstract: | An efficient and practical route to synthesize (2S,3S,4R)‐2‐azido‐3,4‐O‐isopropyllidene‐1,3,4‐octadecanetriol from D‐galactose in 18% overall yield was described, which required ten steps of reactions and only four times column chromatography purification. |
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| Keywords: | glycolipid glycosphingolipid phytosphingosine azidophytosphingosine synthesis |
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