| Synthesis of Unsymmetrical Bissalicylaldimine Ligands and bis-Schiff Base Cobalt Complexes with Benzo-10-aza-15-crown-5 Pendant |
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| 引用本文： | 李建章 徐斌 冯发美 周波 秦圣英. Synthesis of Unsymmetrical Bissalicylaldimine Ligands and bis-Schiff Base Cobalt Complexes with Benzo-10-aza-15-crown-5 Pendant[J]. 中国化学, 2007, 25(11): 1681-1685. DOI: 10.1002/cjoc.200790310 |
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| 作者姓名： | 李建章 徐斌 冯发美 周波 秦圣英 |
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| 作者单位： | [1]Key Laboratory of Green Chemistry, Department of Chemistry, Sichuan University of Science ＆ Engineering, Zigong, Sichuan 643000, China [2]Department of Chemistry, Sichuan University, Chengdu, Sichuan 610064, China |
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| 基金项目： | Prgject supported by the National Natural Science Foundation of China （No. 29572059, and Key Project of Sichuan Province Education 0ffice （No. 2005D007）. |
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| 摘 要： | Novel unsymmetrical bissalicylaldimine bis-Schiff bases with a benzo-10-aza-15-crown-5 pendant and their cobalt complexes have been synthesized via condensation of 3 or 5-[（benzo-10-aza-15-crown-5）-10-ylmethyl] salicylaldehyde with the half unit Schiff bases and characterized by ^1H NMR, IR, mass spectroscopy, elemental analysis, molar conductances and molar magnetic susceptibility.
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| 关 键 词： | 化学合成 缩合 二氧化钴 化学分析 |
| 修稿时间： | 2007-04-30 |
Synthesis of Unsymmetrical Bissalicylaldimine Ligands and bis-Schiff Base Cobalt Complexes with Benzo-10-aza-15-crown-5 Pendant |
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| LI, Jian-Zhang XU, Bina FENG, Fa-Mei ZHOU, Bo QIN, Sheng-Ying. Synthesis of Unsymmetrical Bissalicylaldimine Ligands and bis-Schiff Base Cobalt Complexes with Benzo-10-aza-15-crown-5 Pendant[J]. Chinese Journal of Chemistry, 2007, 25(11): 1681-1685. DOI: 10.1002/cjoc.200790310 |
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| Authors: | LI Jian-Zhang XU Bina FENG Fa-Mei ZHOU Bo QIN Sheng-Ying |
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| Affiliation: | 1. Key Laboratory of Green Chemistry, Department of Chemistry, Sichuan University of Science & Engineering, Zigong, Sichuan 643000, China;2. Department of Chemistry, Sichuan University, Chengdu, Sichuan 610064, China |
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| Abstract: | Novel unsymmetrical bissalicylaldimine bis-Schiff bases with a benzo-10-aza-15-crown-5 pendant and their cobalt complexes have been synthesized via condensation of 3 or 5-[(benzo-10-aza-15-crown-5)-10-ylmethyl] salicylaldehyde with the half unit Schiff bases and characterized by 1H NMR, IR, mass spectroscopy, elemental analysis, molar conductances and molar magnetic susceptibility. |
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| Keywords: | synthesis condensation benzo- 10-aza- 15-crown-5 unsymmetrical bissalicylaldimine bis-Schiff base cobalt complex |
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