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铷和铯含量的示波极谱滴定法测定
引用本文:杨桂株 赵玉清. 铷和铯含量的示波极谱滴定法测定[J]. 分析测试学报, 1998, 17(5): 84-86
作者姓名:杨桂株 赵玉清
作者单位:吉林师范学院理学分院
摘    要:用了示波极谱滴定法测定硝酸盐样品中铷和铯的含量,回收率为9778%~1003%,相对标准偏差均值为021%。该法以示波极谱图形突变来确定滴定终点,终点直观,不受溶液颜色、沉淀的影响,具有准、快、简、省的特点,有广泛的应用价值

关 键 词:示波极谱滴定法,四苯硼钠,铷,铯

Determination of Rubidium and Cesium by Oscillographic Titration
Yang Guizhu,Zhao Yuqing ,Zhan Yongfu. Determination of Rubidium and Cesium by Oscillographic Titration[J]. Journal of Instrumental Analysis, 1998, 17(5): 84-86
Authors:Yang Guizhu  Zhao Yuqing   Zhan Yongfu
Affiliation:Yang Guizhu,Zhao Yuqing *,Zhan Yongfu
Abstract:Rubidium and Cesium in sample of nitrate were determined by oscillographic titration.The end point,being indicated by a sudden change of oscillogram,was not affected by the color of the solution and the precipitation.The recoveries ranged from 97 78% to 100 3% with a RSD of 0 21%.The proposed method proved accurate,precise and simple.
Keywords:Oscillographic titration  Rubidium  Cesium
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