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短链脂肪酸在氧化润滑油涂敷的气相色谱柱上的分离
作者姓名:MOUSTAFANagyEmam
作者单位:Egyptian Petroleum Research Institute, Nasr City, Cairo, Egypt
摘    要:

关 键 词:gaschromatography  lubricatingnaphthenicbaseoil  shortchainfattyacids
  oxidation  
收稿时间:2006-11-15

Separation of Short-Chain Fatty Acids on a Gas Chromatographic Column Coated with Oxidized Lubricating Oil
MOUSTAFANagyEmam.Separation of Short-Chain Fatty Acids on a Gas Chromatographic Column Coated with Oxidized Lubricating Oil[J].Chinese Journal of Chromatography,2007,25(4):606.
Authors:MOUSTAFA Nagy Emam
Institution:Egyptian Petroleum Research Institute, Nasr City, Cairo, Egypt
Abstract:The oxidized lubricating naphthenic base oil was used as a stationary phase for the separation of short-chain free fatty acids (SFFA) either as a pure sample or an aqueous solution containing 0.9 - 1.2 mg/L of each acid. It is found that the oil oxidation for 20 h improved the separation of SFFA in these two sample forms. This separation improvement represents not only the increase in retention volume intervals and peak symmetries in case of the pure sample but also in acid peak areas in case of the aqueous solution sample.
Keywords:oxidation  lubricating naphthenic base oil  gas chromatography  short chain fatty acids
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