| 影响钽探针原子化法测定钐灵敏度原因的实验研究 |
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| 引用本文： | 高云庚,邓勃.影响钽探针原子化法测定钐灵敏度原因的实验研究[J].分析化学,1994,22(6):569-572. |
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| 作者姓名： | 高云庚 邓勃 |
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| 作者单位： | 清华大学化学系!北京100084北京市环境保护监测中心(高云庚)，清华大学化学系!北京100084(邓勃) |
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| 基金项目： | 国家自然科学基金资助项目 |
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| 摘 要： | 用扫描电镜和Ｘ－射线衍射分析研究ＳｍＣｌ３，在钽探针表面原子化时，发现了由于ＳｍＴａＯ４嵌入钽探针而形成镶嵌结构，它影响了测定的灵敏度，并由实验结果说明了衬钽技术的重要性。
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| 关 键 词： | 钽探针 钐 灵敏度 原子化法 |
The Cause for Affecting Sensitivity for the Determination of Samarium in Tantalum Probe Atomization |
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| Gao Yungeng,Deng Bo.The Cause for Affecting Sensitivity for the Determination of Samarium in Tantalum Probe Atomization[J].Chinese Journal of Analytical Chemistry,1994,22(6):569-572. |
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| Authors: | Gao Yungeng Deng Bo |
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| Abstract: | After the determination of samarium using tantalum probe atomization, an intercalation structure was found on the tantalum probe by scanning electron microscopy and X-ray diffraction analysis. The experimental results show that the intercalation structure formed by the intercalation of SmTaO_4 into TaP affected the determination sensitivity . An interpretation for the importance of tantalum foil -lining technique was given according to the experimental results. |
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| Keywords: | Tantalum probe Samarium Intercalation structure |
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