| CRYSTAL STRUCTURE OF [（bpy）2Ru（4,5—DIAZAFLUOREN—9—ONE][PF6]2 |
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| 引用本文： | 朱龙根,杨耀,等.CRYSTAL STRUCTURE OF [（bpy）2Ru（4,5—DIAZAFLUOREN—9—ONE][PF6]2[J].结构化学,1992,11(4):239-243. |
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| 作者姓名： | 朱龙根 杨耀 等 |
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| 摘 要： | <正> V31H22F12N6OP2Ru, Mr = 885.6. Monoclinic, space group P21/n, a=9. 444(4), b = 14.050(7), c=25. 88(1)(?), β=92. 64(4)°, V = 3429.79(?)3, Dc=1. 712gcm-3, F(000) = 1760, μ= 6. 376cm-1, Z = 4, R=0. 077, Rw = 0. 090. There are three different Ru -N bonds of 2. 03(?), 2. 08(?) and 2. 13(?), respectively, to the two bpy and diazafluoren-9-one ligands in the complex.
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| 关 键 词： | 晶体结构 4 5－二氮杂芴酮 钌配合物 |
CRYSTAL STRUCTURE OF [(bpy )_2Ru ( 4, 5-DIAZAFLUOREN-9-ONE][PF_6]_2 |
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| Institution: | [1]CoordinationChemistryInstituteofNanjingUniversity, [2]CoordinationChemistryInstitut, |
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| Abstract: | V31H22F12N6OP2Ru, Mr = 885.6. Monoclinic, space group P21/n, a=9. 444(4), b = 14.050(7), c=25. 88(1)(?), β=92. 64(4)°, V = 3429.79(?)3, Dc=1. 712gcm-3, F(000) = 1760, μ= 6. 376cm-1, Z = 4, R=0. 077, Rw = 0. 090. There are three different Ru -N bonds of 2. 03(?), 2. 08(?) and 2. 13(?), respectively, to the two bpy and diazafluoren-9-one ligands in the complex. |
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