| OV—210弹性石英毛细管柱交联方法研究 |
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| 引用本文： | 曾昭睿 吴采樱. OV—210弹性石英毛细管柱交联方法研究[J]. 分析化学, 1992, 20(11): 1349-1354 |
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| 作者姓名： | 曾昭睿 吴采樱 |
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| 作者单位： | 武汉大学化学系，武汉大学化学系，武汉大学化学系化学系分析专业 武汉 430072，武汉 430072，85级本科生 武汉 430072 |
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| 摘 要： |
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| 关 键 词： | 毛细管柱 交联 偶氮特丁烷 DCUP |
Crosslinking Methods of the OV-210 Stationary Phase on Fused Silica Capillary Columns |
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| Zeng Zhaorui,Wu Caiying,Li Baoshan. Crosslinking Methods of the OV-210 Stationary Phase on Fused Silica Capillary Columns[J]. Chinese Journal of Analytical Chemistry, 1992, 20(11): 1349-1354 |
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| Authors: | Zeng Zhaorui Wu Caiying Li Baoshan |
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| Affiliation: | Zeng Zhaorui~*,Wu Caiying,Li Baoshan |
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| Abstract: | Three crosslinking methods of the OV-210 stationary phase on fused silica capillary columns were studied and their chromatographic performances were evaluated. The optimal crosslinking condition and the possible mechanism were discussed. It showed that the separation efficiency and the thermal stability were good, and columns had only minor shift in polarity after the curing. It demonstrated that the columns crosslinked with dicumyl peroxide, ozone as initiators were better than those with azo tert-butane while the latter had higher column efficiency. |
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| Keywords: | Capillary Crosslink Dicumyl peroxide Ozone Azo tert-butane |
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