Synthesis, characterization, and crystal structure of 1-(4-chloro-benzoyl)-3-naphthalen-1-yl-thiourea |
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| Authors: | Hakan Arslan Ulrich Flörke Nevzat Külcü |
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| Affiliation: | (1) Department of Chemistry, Faculty of Arts and Sciences, Mersin University, 33343 Mersin, Turkey;(2) School of Chemistry and Biochemistry, Georgia Institute of Technology, Atlanta, Georgia;(3) Department of Inorganic and Analytical Chemistry, University of Paderborn, Paderborn, Germany |
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| Abstract: | 1-(4-Chloro-benzoyl)-3-naphthalen-1-yl-thiourea has been synthesized and characterized by elemental analysis, IR spectroscopy, and mass spectrometry. The crystal and molecular structure of the title compound has been determined from single crystal X-ray diffraction data. It crystallizes in the triclinic space group P-1, with a = 6.962(1) Å, b = 10.770(3) Å, c = 11.738(2) Å,  = 65.76(2)°,  = 80.03(1)°,  = 84.86(2)°, and Dcalc= 1.432 g cm–1 for Z = 2. The thermal behavior of the compound has been studied by DTA and TG. The antibacterial activities of the title compound were investigated for three Gram (+) and two Gram (–) bacteria by employing broth microdilution method and subsequently, inhibitory activity against yeast-like fungi was also determined. |
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| Keywords: | Thioureas synthesis X-ray structures DTA/TG antibacterial activities |
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