| 电感耦合等离子体原子发射光谱法测定电解金属锰中硒、铁、硅 |
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| 引用本文： | 方红,杨晓兵. 电感耦合等离子体原子发射光谱法测定电解金属锰中硒、铁、硅[J]. 光谱学与光谱分析, 2001, 21(3): 373-376 |
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| 作者姓名： | 方红 杨晓兵 |
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| 作者单位： | 山西出入境检验检疫局技术中心 |
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| 摘 要： | 本文采用稀硫酸溶解试样，ICP－AES法同时测定电解金属锰中硒、铁、硅，通过对溶样酸、锰基体以及背景的研究，确定了分析条件。该方法简便具有良好的精密度和准确性，相对标准偏差不大于2．68％，回收率为98％－105％。经t检验与经典法无显著性差异。
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| 关 键 词： | 电解金属锰 ICP－AES 硒 铁 硅 测定 电感耦合等离子体原子发射光谱法 |
| 修稿时间： | 2000-05-29 |
Determination of Se,Fe,Si in Electrolytic Manganese Metal by ICP-AES |
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| H Fang,X Yang. Determination of Se,Fe,Si in Electrolytic Manganese Metal by ICP-AES[J]. Spectroscopy and Spectral Analysis, 2001, 21(3): 373-376 |
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| Authors: | H Fang X Yang |
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| Affiliation: | Shangxi Entry-Exit Inspection and Quarantine Bureau, 030024 Taiyuan. |
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| Abstract: | The method was established for the simultaneous determination of Se, Fe and Si in electrolytic manganese metal by inductively coupled plasma atomic emission spectrometry (ICP-AES). The sample was dissolved by light sulphuric acid. The analysis conditions were obtained by studying dissolved acid, Mn matrix and background. The recommended method not only proved to be simple and rapid but showed satisfying precision and accuracy as well. The relative standard deviation is less than 2.68% and the recovery is 98%-105%. The t-test showed that no conspicuous difference with typical methods was found. |
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| Keywords: | Electrolytic manganese metal ICP AES Selenium Iron Silicon |
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