GC-MS analysis of dichlobenil and its metabolites in groundwater |
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Authors: | Porazzi E Pardo Martinez M Fanelli R Benfenati E |
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Affiliation: | Department of Environmental Health, Sciences for Pharmacological Research “Mario Negri” Institute, Via Eritrea 62, 20157 Milano, Italy |
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Abstract: | We have developed a new method for the determination of the widely used herbicide 2,6-dichlorobenzonitrile (dichlobenil) and its major metabolites 2,6-dichlorobenzamide (BAM) and 2,6-dichlorobenzoic acid (2,6-DCBA) in groundwater samples. The procedure is based on solid phase extraction (SPE) combined with a derivatization procedure before GC-MS analysis in order to quantify analytes simultaneously. This method can be used from regulatory laboratories for monitoring the presence of dichlobenil and its metabolites during testing groundwater samples quality. |
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Keywords: | Water Pesticides Metabolites Monitoring GC-MS |
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