合金钢光谱分析通用方法

本文介绍利用溶液法和粉末法进行合金钢光谱分析的方法,以克服制备标准样品的困难和消除样品组织结构和物理状态的影响。将钢样溶解于酸制成的溶液,滴在平头碳电极上用火花激发,或将钢样制成氧化物粉末,填于碳孔中,用交流电弧激发。初步结果指出,这些方法可以满足一般分析要求。

UNIVERSAL METHODS FOR THE SPECTROCHEMICAL ANALYSIS OF ALLOY STEELS

In order to simplify the preparation of standards and to reduce the effects of micro-structure and physical state of samples in the spectrochemical analysis of alloy steels, universal methodg are developed in this laboratory. For the solution method, steel samples dissolved in acid and dropped on the flat tip of carbon electrodes are excited in a spark source. For the powder method, oxides prepared from the steel samples are put in cavities of carbon electrodes and excited in an a. c. are. Experiments show that these procedures give satisfactory analytical results.