| 自动快速燃烧炉-离子色谱联用技术检测水泥等建材中的氯 |
| |
| 引用本文： | 王碗,刘肖,蔡亚岐,牟世芬. 自动快速燃烧炉-离子色谱联用技术检测水泥等建材中的氯[J]. 分析试验室, 2007, 26(12): 10-13 |
| |
| 作者姓名： | 王碗 刘肖 蔡亚岐 牟世芬 |
| |
| 作者单位： | 中国科学院生态环境研究中心,环境化学与生态毒理学国家重点实验室,北京,100085;北京理工大学生命科学与技术学院,北京,100081;中国科学院生态环境研究中心,环境化学与生态毒理学国家重点实验室,北京,100085 |
| |
| 基金项目： | 国家重点基础研究发展计划(973计划) , 中国科学院科研基金 |
| |
| 摘 要： | 建立了一种全新的以燃烧方法处理固体样品的装置——自动快速燃烧炉(AQF)与离子色谱联用的技术,检测建筑材料中氯的方法.该方法将AQF的快速处理样品的能力和离子色谱的准确性好、灵敏度高的特点相结合,可以连续批量处理样品,平均在18 min之内完成一个样品的检测.方法的线性、重现性、检测限均令人满意.还进行了水提法处理待测样品,将其结果与AQF处理的结果相比较,结果表明AQF处理的方法具可行性.
|
| 关 键 词： | AQF 离子色谱 燃烧 建材 氯 |
| 文章编号： | 1000-0720（2007）12-010-04 |
| 收稿时间： | 2006-09-15 |
| 修稿时间： | 2006-12-05 |
Determination of chloride in some building materials by automatic quick furnace-ion chromatography |
| |
| WANG Wan,LIU Xiao,CAI Ya-qi,MOU Shi-fen. Determination of chloride in some building materials by automatic quick furnace-ion chromatography[J]. Chinese Journal of Analysis Laboratory, 2007, 26(12): 10-13 |
| |
| Authors: | WANG Wan LIU Xiao CAI Ya-qi MOU Shi-fen |
| |
| Abstract: | The present paper developed a new method to analyse chloride in building materials such as cement by combining a new instrument named automatic quick furnace(AQF) which can do the preparation of solid samples by burning and ion chromatography together.This method exerts the abilities of AQF which can treat sample fast and the advantages of ion chromatography.We only need 18 minutes to treat a single sample on average by AQF-IC.The linear range,RSD,detection limit and recoveries of this method are all satisfactory.On the other hand,we extracted the sample with DI water and measured the solution by suppressed ion chromatography.The results by the later method are not as good as those by AQF-IC. |
| |
| Keywords: | AQF Ion chromatography Burning Building materials Chloride |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
