Determination of melamine in milk powder using gas chromatography-high-resolution isotope dilution mass spectrometry |
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Authors: | Koh Guiwan Chia Rosalind S C Lin Qi Cheow Pui-Sze Teo Tang-Lin Lee Tong-Kooi |
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Affiliation: | Health Sciences Authority, Chemical Metrology Division, Chemical Metrology Laboratory, The Capricorn, Singapore Science Park II, Singapore. |
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Abstract: | A GC-high-resolution isotope dilution MS (IDMS) method for the quantification of melamine in milk powder is described. The developed technique is compared to the LC-IDMS/MS technique, typically used for the determination of melamine in various matrices. The accuracy of the GC-high-resolution IDMS method was demonstrated when a small degree of equivalence was obtained in a regional comparative study involving the determination of melamine in milk powder. |
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Keywords: | GC High resolution isotope dilution MS Melamine Milk powder |
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