Electrochemical synthesis of pentamethylenediazirine |
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| Authors: | M. D. Vedenyapina V. V. Kuznetsov E. A. Nizhnikovskii E. D. Strel’tsova N. N. Makhova M. I. Struchkova A. A. Vedenyapin |
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| Affiliation: | (1) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991 Moscow, Russian Federation;(2) Interdepartment Scientific Council on Complex Problems of Physics Chemistry, and Biology at the Presidium of the Russian Academy of Sciences, 5 ul. Dm. Ul’yanova, 119333 Moscow, Russian Federation |
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| Abstract: | Electrochemical synthesis of pentamethylenediazirine at the Pt/Ti anode was conducted. The reaction is reversible. The rate constants of the direct and reverse processes were estimated. The product and current yields of the target compound approach to 100%. Dedicated to Academician O. M. Nefedov on the occasion of his 75th birthday. Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 1939–1941, November, 2006. |
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| Keywords: | pentamethylenediazirine pentamethylenediaziridine electrochemical synthesis |
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