Microwave synthesis of core-shell gold/palladium bimetallic nanoparticles |
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Authors: | Harpeness Riki Gedanken Aharon |
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Institution: | Department of Chemistry, Bar-Ilan University, Ramat-Gan 52900, Israel. |
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Abstract: | The microwave-assisted polyol reduction method was applied to the synthesis of core-shell gold/palladium bimetallic nanoparticles by the simultaneous reduction of the AuIII and PdII ions. The thickness of the palladium shell was calculated to be approximately 3 nm, and the gold core diameter is 9 nm. The structure and composition of the bimetallic particles were characterized by high-resolution transmission electron microscopy equipped with a nanoarea energy-dispersive X-ray spectroscopy attachment, transmission electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. |
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