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Characterisation of Screen-Printed Electrodes for Detection of Heavy Metals
Authors:I. Palchetti  A. Cagnini  M. Mascini  A. P. F. Turner
Affiliation:(1)  Dipartimento di Sanità Pubblica, Epidemiologia, e Chim. Anal. Ambientale, Università degli studi di Firenze, Via Gino Capponi 9, 50121 Firenze, Italy, IT;(2)  Cranfield Biotechnology Centre, Cranfield University, Bedfordshire, MK430AL,
Abstract: The characterisation of disposable screen-printed electrodes for stripping analysis is described. The graphite surface of the working electrode is used as substrate for plating a thin mercury film, which allows the electrochemical preconcentration of heavy metals. Optimisation procedures and experimental results are presented. Detection limits around the ppb level were obtained for different metals [Pb(II), Cd(II), Cu(II)]. Received June 6, 1998. Revision November 10, 1988.
Keywords::   screen-printed electrodes   heavy metals   anodic stripping voltammetry   potentiometric stripping analysis.
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