Spectroscopic studies and crystal structure of tetrabutylammonium trichlorodimethylstannate(IV): Bu4NSnMe2Cl3 |
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| Institution: | 1. Laboratoire de chimie minérale et analytique (LACHIMIA), département de chimie, faculté des sciences et techniques, université Cheikh-Anta-Diop de Dakar, Dakar, Sénégal;2. Instituto de Chimica, Universidad National Autonoma de Mexico, Circuito Exterior, Ciudad Universitaria, Mexico D.F. 04510, Mexico;3. Département de chimie, CPMC, place Louis-Pasteur, B-1348 Louvain-la-Neuve, Belgique |
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| Abstract: | The structure of Bu4NSnMe2Cl3 is found to be monomer, containing a 5-coordinated bipyramidal trigonal tin(IV) center. Crystals belong to the monoclinic space group C2/c, with unit-cell dimensions a = 26.633(4) Å; b = 9.880(2) Å; c = 21.510(2) Å; β = 114.82(2)°; Z = 8; D = 1.287 Mg/m3; R is refined to 0.0537 and Rw = 0.0642 for 3330 reflections (F > 2σ(F)). |
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