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Synthesis and Characterization of Tris(diethyldithiocarbamato) cobalt(III) as an Undergraduate Inorganic Laboratory
Authors:C T Eagle  D G Farrar  G N Holder  D M Gooden  A B Goodman  S W Wyatt
Institution:(1) Department of Chemistry, Appalachian State University, Boone, NC, 28608
Abstract:The synthesis of tris(diethyldithiocarbamato) cobalt(III) by the reaction of sodium diethyldithio-carbamate and cobaltous chloride is described. The recovered crystals of the cobalt complex are characterized by magnetic susceptibility, IR and NMR spectroscopy, and cyclic voltammetry.
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