| 1,3-二环基碳化二亚胺催化的阿魏酸对硝基苯酚酯一步合成法 |
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| 引用本文： | 韦长梅,徐斌,朱红军,王锦堂. 1,3-二环基碳化二亚胺催化的阿魏酸对硝基苯酚酯一步合成法[J]. 应用化学, 2004, 21(11): 1184-1186 |
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| 作者姓名： | 韦长梅 徐斌 朱红军 王锦堂 |
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| 作者单位： | 南京工业大学 |
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| 基金项目： | 江苏省社会发展基金(BS2002041)资助项目 |
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| 摘 要： | 1;3-二环基碳化二亚胺催化的阿魏酸对硝基苯酚酯一步合成法;酯化反应
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| 关 键 词： | 3-二环基碳化二亚胺催化的阿魏酸对硝基苯酚酯一步合成法 酯化反应 |
| 文章编号： | 1000-0518(2004)11-1184-03 |
| 收稿时间： | 2009-06-29 |
| 修稿时间： | 2003-12-15 |
One-step Synthesis of 4-Nitrophenyl Ferulate in Presence of DCC as Catalyst |
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| WEI Chang Mei,XU Bin,ZHU Hong Jun,WANG Jin Tang. One-step Synthesis of 4-Nitrophenyl Ferulate in Presence of DCC as Catalyst[J]. Chinese Journal of Applied Chemistry, 2004, 21(11): 1184-1186 |
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| Authors: | WEI Chang Mei XU Bin ZHU Hong Jun WANG Jin Tang |
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| Affiliation: | WEI Chang Mei,XU Bin,ZHU Hong Jun,WANG Jin Tang * |
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| Abstract: | Nitrophenyl ferulate was synthesized in one step without the protection of the hydroxyl of ferulic acid in the presence of 1,3 dicyclohexylcarbodiimide(DCC) as the catalyst. Thus, 15 20 g of ferulic acid reacted with 18 07 g of 4 nitrophenol for 24 h at room temperature in the presence of 22 44 g of DCC. The crude product was recrystallized from CHCl 3 to give 16 00 g of 4 nitrophenyl ferulate and the yield was 82 5%. Elemental analysis, IR and 1H NMR techniques were used to prove the structure of the product. |
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| Keywords: | nitrophenyl ferulate dicyclohexylcarbodiimide catalystic esterification |
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