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Determination of Traces of Toxic Elements in Dimethylaminoborane upon Their Concentration for Atomic Emission Analysis
Authors:R. V. Lebedeva  N. N. Vyshinskii  A. N. Tumanova  N. I. Mashin
Affiliation:(1) Scientific-Research Institute of Chemistry at the, N. I. Lobachevskii Nizhnii Novgorod State University, 23 Gagarin Ave., Nizhnii Novgorod, 603095, Russia
Abstract:A technique of atomic emission determination of traces of toxic elements in dimethylaminoborane with detection limits of n·10–5–10–8 wt. % has been developed. To reduce the detection limits, a technique of separation of the basic component in the form of boron fluoride, with concentration of microimpurities on a graphite collector, was used.
Keywords:atomic emission analysis  arc excitation  photographic recording  dimethylaminoborane  matrix effect  graphite collector
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