Application of Microflame Atomizer to Gas Chromatography-Atomic Absorption Spectrometry |
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Authors: | SUN Jian-Min YAN Zheng LIU Li-Ping ZHANG De-Qiang YANG Li-Li SUN Han-Wen |
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Institution: | Department of Chemistry, Hebei University, Baoding, 071002, P. R. China |
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Abstract: | One of the successful methods for the determination of organometallic compounds is the combination of Gas Chromatography-Atomic Absorption Spectrometry (GC-AAS). The atomizer of AAS was connected with the column of GC by a transfer tube. Three types of the atomizer were reported as flame burner,electrothermal quartz tube and graphite furnace. A large amount of gas or electric energy was required to produce a high temperature for the atomization of analytes, A microflame atomizer of GC-AAS was developed in this paper to circumvent above problems. The volume of the atomizer is one-fifth of the normal flame burner, and a hydrogen gas was used as the carrier gas (35ml/min) and the fuel gas for the atomization of analytes. |
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