14个N-取代苯基-N'-[6-(2-取代苯并噻唑)基]脲类化合物的 合成与结构表征 |
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引用本文: | 李再峰,罗富英.14个N-取代苯基-N'-[6-(2-取代苯并噻唑)基]脲类化合物的 合成与结构表征[J].有机化学,2001,21(4):317-321. |
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作者姓名: | 李再峰 罗富英 |
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作者单位: | 湛江师范学院科技开发中心 |
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基金项目: | 广东省粤高教科[1999]89资助项目. |
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摘 要: | 为了寻找新的高活性植物调节品种,以苯并噻唑,2-甲基苯并噻唑和取代苯胺为原料合成了7个N-取代苯基-N'(6-苯并噻唑基)脲和7个N-取代苯基一N'-6-(2-甲基苯并噻唑)基]脲类新化合物,其产率分别为74.0%、76.0%、85.0%、82.0%、70.0%、73.0%、72.0%、82.0%、88.5%、87.0%、90.5%、91.0%、83.5%和85.0%。14个脲类化合物结构经元素分析、IR和1HNMR表征。各化合物的植物细胞分裂性被初步测定。
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关 键 词: | 苯基 脲 异氰酸酯 苯并噻唑P 结构表征 植物生长调节剂 合成法 |
修稿时间: | 2000年10月23 |
Synthesis and structure characterization of 14 N- substituted phenyl- N'-[6-(2-substituted benzothiazol)yl] urea compounds |
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Abstract: | Seven N-substituted phenyl-N'-(6-benzothiazoly)-and seven N- substituted phenyl-N'-6-(2-methyl-benzothiazol)yl] ureas were synthesized in 70.0% ~ 91.0% yields by a series of reaction of benzothiazole and 2-methyl-benzothiazole with substituted phenylamines, respectively, in search of new compounds with plant growth regulation activity. The structures of fourteen compounds were characterizated by elemental analysis、 IR and 1^H NMR. Preliminary cytokinin-activity of the compounds were determined. |
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Keywords: | PHENYL GROUP UREA ISOCYANIC ESTERS BENZOTHIAZOLE P STRUCTURE CHARACTERISTICS PLANT GROWTH REGULATORS SYNTHESIS METHODS |
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