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在钛酸钠纤维表面吸附生长SnO_2量子点
引用本文:韦志仁,彭翔宇,张利明,周阳,董国义. 在钛酸钠纤维表面吸附生长SnO_2量子点[J]. 人工晶体学报, 2009, 38(6): 1438-1441
作者姓名:韦志仁  彭翔宇  张利明  周阳  董国义
作者单位:河北大学物理科学与技术学院,河北省光电信息材料重点实验室,保定,071002
摘    要:本文研究了水热条件下SnO_2纳米晶体在钛酸钠纤维表面的吸附生长特性.采用水热法,以钛酸钠晶体纤维和适量的SnCl_4· 5H_2O为前驱物,水热反应条件为pH值11,填充度68;,反应温度120 ℃、150 ℃,反应时间24 h,在钛酸钠纤维表面生长了金红石相SnO_2纳米晶体,晶体尺度约为5 nm.实验结果显示钛酸钠晶体表面具有很强的表面活化能.

关 键 词:水热法  纳米晶体  钛酸钠  二氧化锡,

Adsorption Growth of SnO_2 Quantum Dot on the Surface of Sodium Titanate Crystal Fibers
WEI Zhi-ren,PENG Xiang-yu,ZHANG Li-ming,ZHOU Yang,DONG Guo-yi. Adsorption Growth of SnO_2 Quantum Dot on the Surface of Sodium Titanate Crystal Fibers[J]. Journal of Synthetic Crystals, 2009, 38(6): 1438-1441
Authors:WEI Zhi-ren  PENG Xiang-yu  ZHANG Li-ming  ZHOU Yang  DONG Guo-yi
Abstract:In this paper, the adsorption growth characteristics of SnO_2 nanocrystals grown on the surface of sodium titanate crystal fibers were investigatived. The rutile structure SnO_2 nano-crystals quantum dot have been prepared on the surface of sodium titanate crystal fibers by the hydrothermal method using sodium titanate crystal fibers and proper amount of SnCl_4· 5H_2O as the precursors. The reaction conditions was pH value 11, the fill factor was 68%, reacting temperature were 120 ℃ and 150 ℃ respectively, the total reacting time was 24 h. The SnO_2 nano-crystals had a size of about 5 nm. The results show that the surface of sodium titanate had a strong apparent activation energy.
Keywords:hydrothermal method  nano-crystals  sodium titanate  SnO_2
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