A convenient synthesis of (1S)-tert-butyl-1,2-ethylenediamine |
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| Affiliation: | 1. State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, Liaoning China;2. University of Chinese Academy of Sciences, Beijing 100049, China;1. Southern Federal University, Institute of Physics, Stachki ave. 194, 344090, Rostov-on-Don, Russian Federation;2. Southern Federal University, Institute of Physical and Organic Chemistry, Stachki ave. 194/2, 344090, Rostov-on-Don, Russian Federation;3. Siberian Branch of the Russian Academy of Sciences, Boreskov Institute of Catalysis, Lavrentiev Ave. 5, 630090, Novosibirsk, Russian Federation;4. National Research Center «Kurchatov Institute», Acad. Kurchatov Sq. 1, 123182, Moscow, Russian Federation;5. Peoples’ Friendship University of Russia (RUDN University), Miklukho-Maklaya ul. 6, 117198, Moscow, Russian Federation;6. N. D. Zelinsky Institute of Organic Chemistry RAS, Leninsky Prosp. 47, 119991, Moscow, Russian Federation;1. Department of Nano Fusion Technology and BK21 Plus Nano Convergence Technology Division, Pusan National University, Busan 609-735, Republic of Korea;2. Department of Nanoenergy Engineering, Pusan National University, Busan 609-735, Republic of Korea |
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| Abstract: | A practical four-step synthesis of (1S)-tert-butyl-1,2-ethylenediamine has been developed. The sequence proceeds in good overall yield via crystalline intermediates and provides the title compound in 99.3% ee. |
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