Single-step thioetherification by indium-catalyzed reductive coupling of carboxylic acids with thiols |
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| Authors: | Norio Sakai Takahiro Miyazaki Tomohiro Sakamoto Takuma Yatsuda Toshimitsu Moriya Reiko Ikeda Takeo Konakahara |
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| Institution: | Department of Pure and Applied Chemistry, Faculty of Science and Technology, Tokyo University of Science (RIKADAI) , Noda, Chiba 278-8510, Japan. |
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| Abstract: | Direct thioetherification from a variety of aromatic carboxylic acids and thiols using a reducing system combined with InBr(3) and 1,1,3,3-teramethyldisiloxane (TMDS) in a one-pot procedure is demonstrated. It was also found that a system combined with InI(3) and TMDS underwent thioetherification of aliphatic carboxylic acids with thiols. |
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