Regeneration of ketones from semicarbazones by lead tetra-acetate: A novel preparation of 18-hydroxycorticosterone |
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| Authors: | David N Kirk Christopher J Slade |
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| Institution: | Medical Research Council Steroid Reference Collection, Chemistry Department, Westfield College, Hampstead, London, NW3 7ST, U.K. |
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| Abstract: | Lead tetra-acetate in acetic acid has been used to cleave a 3-semi-carbazone in a novel preparation of 18-hydroxycorticosterone, designed to avoid strongly acidic conditions. |
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