Über die Darstellung der N-Chlor-N-Methylammoniumsalze (CH3)nNCl4–n+MF6− (n = 1–3; M = As,Sb) und (CH3)2NCIX+MF6− (X = F,Br) |
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Authors: | R. Minkwitz D. Bernstein P. Sartori |
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Abstract: | About the Preparation of N-Chloro-N-Methylammonium Salts (CH3)nNCl4–n+MF6? (n = 1–3; M = As, Sb) and (CH3)2NClX+MF6? (X = F, Br) Simple one-step methods for the preparation of the methylated chloroammonium salts (CH3)nNCl4–n+MF6? (n = 1–3; M = As, Sb) and for (CH3)2NClX+MF6? (X = F, Br) are reported. Their vibrational and NMR-spectroscopical data are discussed in comparison. |
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Keywords: | N-chloro-N-methylammonium hexafluoroarsenate, -stibate syntheses i.r., n.m.r. spectra |
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