Synthesis and spectral properties of [3-(heptyloxy)phenoxy]acetic acid and its derived meso-sibstituted tetrabenzoporphyrins |
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Authors: | N. E. Galanin L. A. Yakubov G. P. Shaposhnikov |
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Affiliation: | (1) Ivanovo State Chemical Technological University, pr. F. Engel’sa 7, Ivanovo, 153000, Russia |
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Abstract: | 3-Heptyloxyphenol was obtained by reaction of resorcinol with 1-bromoheptane. Further alkylation with monochloroacetc acid resulted in the synthesis of [3-(heptyloxy)phenoxy]acetic acid. Heating of the latter with phthalimide in the presence of zinc acetate afforded zinc complexes of meso-[(3-heptyloxy)phenoxy] tetrabenzoporphyrins whose demetalization gave free porphyrin bases. Spectral properties of the synthesized compounds were studied. |
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