| Iodine Supported on 3-Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent-free Conditions |
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| 引用本文： | MAHDAVI Hossein,GHAEMY Mosa,ZERAATPISHEH Fatemeh. Iodine Supported on 3-Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent-free Conditions[J]. 中国化学, 2009, 27(2): 347-352. DOI: 10.1002/cjoc.200990056 |
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| 作者姓名： | MAHDAVI Hossein GHAEMY Mosa ZERAATPISHEH Fatemeh |
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| 作者单位： | a School of Chemistry, University College of Science, University of Tehran, P. O. Box 14155-6455, Tehran, Iran ;b Department of Chemistry, University of Mazandaran, Babolsar, Iran ; |
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| 摘 要： | 3-Aminopropyl silica gel (I2/APSG) was found to catalyze the acetylation of alcohols and phenols efficiently with acetic anhydride. The reaction is mild and selective with high yields. A wide variety of alcohols and phenols are selectively converted into the corresponding acetates using I2/APSG under solvent-free conditions at room temperature.
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| 关 键 词： | iodine 3-aminopropyl silica gel acetylation alcohol |
| 收稿时间： | 2008-01-03 |
| 修稿时间： | 2008-05-07 |
Iodine Supported on 3-Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent-free Conditions |
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| MAHDAVI Hossein,GHAEMY Mosa,ZERAATPISHEH Fatemeh. Iodine Supported on 3-Aminopropyl Silica Gel as Efficient Catalyst for Acetylation of Alcohols under Solvent-free Conditions[J]. Chinese Journal of Chemistry, 2009, 27(2): 347-352. DOI: 10.1002/cjoc.200990056 |
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| Authors: | MAHDAVI Hossein GHAEMY Mosa ZERAATPISHEH Fatemeh |
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| Abstract: | 3‐Aminopropyl silica gel (I2/APSG) was found to catalyze the acetylation of alcohols and phenols efficiently with acetic anhydride. The reaction is mild and selective with high yields. A wide variety of alcohols and phenols are selectively converted into the corresponding acetates using I2/APSG under solvent‐free conditions at room temperature. |
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| Keywords: | iodine 3‐aminopropyl silica gel acetylation alcohol |
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