Oxidative methods for synthesis ofα,α′-dioxygen-containing derivatives of dehydrodesthiobiotin |
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Authors: | S I Zav'yalov N A Rodionova E P Gracheva |
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Institution: | (1) N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, USSR |
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Abstract: | Conclusions The action of selenium dioxide in dioxane on the ethyl ester of -ketodebydrodesthiobiotin and of lead tetraacetate in glacial acetic acid on its N,N -diacetyl derivative give the corresponding ethyl esters of ,![agr](/content/l52t2814h0g32mkm/xxlarge945.gif) -dioxodehydrodesthiobiotin and -oxo-![agr](/content/l52t2814h0g32mkm/xxlarge945.gif) -acetoxy-N,N -diacetyldehydrodesthiobiotin.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 9, pp. 2025–2028, September, 1972. |
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