Gansu Key Laboratory of Polymer Materials, College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, Gansu 730070, PR China
Abstract:
Silica sulfate has been proved to be an efficient and recyclable catalyst for Beckmann rearrangement of a variety of oximes in acetone under microwave irradiation. This protocol has advantages of high conversion, high selectivity, short reaction time, no environmental pollution, and simple work-up procedure.