The synthesis and characterization of pure substance reference materials for forensic, agricultural and drugs-in-sport analysis |
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| Authors: | Bruce Noble |
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| Institution: | (1) Pure Substance Reference Materials Team, National Analytical Reference Laboratory, P. O. Box 385 Pymble, NSW 2073, Australia Tel.: +61-2-9449-0111 Fax: +61-2-9449-1653 e-mail: bruce.noble@agal.gov.au, AU |
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| Abstract: | The paper reports work on the synthesis, purification and certification of pure substance (organic) reference materials as
conducted within the National Analytical Reference Laboratory (NARL). Areas of interest include illicit drugs, agricultural
and veterinary chemicals, and steroids and steroid metabolites and their deuterates. The discussion covers the prioritization
of work requirements, procedures for synthesis and production, quality assurance, characterization, homogeneity, storage and
stability testing, and certification of materials. Future plans for establishing traceability are also discussed. |
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| Keywords: | Pure substance reference materials Characterization Certification Quality assurance and control Purification |
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