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Tracing of dislocations in ammonium hydrogen tartrate single crystals
Authors:C C Desai  A N Hanchinal
Abstract:Sparingly soluble ammonium hydrogen tartrate (AHT) crystals are grown by the gel method, derived from the diffusion of ammonium chloride into the set gel containing tartaric acid. Crystals up to 23 × 5 × 3 mm3 in size are grown at room temperature. AHT crystals are cleaved along (010) planes and the cleavage surfaces are studied by using multiple beam interferometry. The interferograms have revealed that the cleavages are quite flat. An attempt is made to trace the trajectory of dislocations of isolated as well as matched pairs of (010) cleavages of AHT when etched in a mixture of formic acid and methyl alcohol (2:1) and 1.0 M SrCl2 solutions. Optical and transmission electron micrographs of dislocations show oblique, parallel and continuous line characteristics. Rows of equally spaced dislocation pits are observed and the implications of this are discussed.
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