摘 要: | ThefactthathypophosphiteisoneofthemostwidelyusedreducingagentsintheNielectrolessdepositionhasstimulatedthestudyofanodicoxidationofhypophosphiteonnicked-ic.Thisanodicreaction,whichisimportantfortheunderstandingoftheNielectrolessdepositionmechanism,isexpectedtobeoneoftheimportantreactionsintheNi-electrolessprocess.Recently,theroleandoxidationmechanismofhypophosphiteinelectrolessdepositionofNi-Palloyhavebeenstudiedindetailusingtheprobebeamdeflection',electrochemistryandinsituIR',lo.However,som…
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