Abstract: | Various optical techniques have been investigated as potential candidates for characterization of multiphase polymeric materials. The model calculations and corresponding experiments (time‐resolved light scattering and image analysis) have been conducted to investigate the kinetics of phase dissolution of polymer blends. The blends studied were polystyrene/poly (methyl methacrylate) mixtures with diblock copolymer composed of the corresponding homopolymers. The time evolution of the spinodal peak position qm(t,T) and the scattered intensity maximum Im(t,T) at qm have been compared with theoretically predicted values of exponents for distinct time scales of the phase dissolution in various temperature regimes. |