| 固相萃取-高效液相色谱法测定烟叶中吡虫啉农药残留量 |
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| 引用本文： | 师君丽,宋春满,方敦煌,逄涛,刘彦红. 固相萃取-高效液相色谱法测定烟叶中吡虫啉农药残留量[J]. 光谱实验室, 2012, 29(1): 83-86 |
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| 作者姓名： | 师君丽 宋春满 方敦煌 逄涛 刘彦红 |
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| 作者单位： | 云南省烟草农业科学研究院分析测试中心 653100 |
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| 基金项目： | 中国烟草总公司云南省公司科技计划项目 |
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| 摘 要： | 建立了固相萃取-高校液相色谱法测定烟叶中吡虫啉农药残留量的方法。样品用乙腈提取,弗罗里硅土固相萃取柱净化.梯度洗脱方式分离,DAD二极管阵列检测器检测。吡虫啉加标回收率为87.83%—94.80%,相对标准偏差为1.64%,检出限为0.01μg/g。该方法灵敏、准确,适用烟草中吡虫啉农药残留的分析。
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| 关 键 词： | 吡虫啉 固相萃取 高效液相色谱 烟叶 |
Determination of Imidacloprid Residue in Tobacco by High Performance Liquid Chromatography with Solid-Phase Extraction |
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| SHI Jun-Li , SONG Chun-Man , FANG Dun-Huang , PANG Tao , LIU Yan-Hong. Determination of Imidacloprid Residue in Tobacco by High Performance Liquid Chromatography with Solid-Phase Extraction[J]. Chinese Journal of Spectroscopy Laboratory, 2012, 29(1): 83-86 |
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| Authors: | SHI Jun-Li SONG Chun-Man FANG Dun-Huang PANG Tao LIU Yan-Hong |
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| Affiliation: | (Analysis and Testing Center,Yunnan Academy of Tobacco Agricultural Sciences,Yuxi,Yunnan 653100,P.R.China) |
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| Abstract: | A method for the determination of imidacloprid residue in tobacco leaves by high performance liquid chromatography with solid-phase extraction with DAD detector was established. Tobacco samples were extracted with acetonitrile and cleaned up with a florisil SPE column,then separated in a gradient elution mode.The results showed that the average recoveries of imidacloprid were in the range of 87.83%—94.80%with relative standard deviation of 1.64%,and the limit of detection was 0.01μg/g.The method is sensitive and suitable for the analysis of imidacloprid residue. |
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| Keywords: | Imidacloprid Solid-Phase Extraction HPLC Tobacco Leaf |
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