Synthesis,structure, and transformations of 1-aza-3-oxa-7-thiabicyclo[3.4.0]nonan-2-one |
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| Authors: | A V Eremeev R Nurdinov F D Polyak R M Zolotoyabko A F Mishnev S V Belyakov Ya Ya Bleidelis |
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| Institution: | (1) Institute of Organic Synthesis, Academy of Sciences of the Latvian SSR, 226006 Riga |
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| Abstract: | 1-Aza-3-oxa-7-thiabicyclo3.4.0]nonan-2-one was obtained by reduction of 3,4-dimethoxycarbonyltetrahydro-1,4-thiazine. The reduction of this product with lithium aluminum hydride led to 3-hydroxymethyl-4-methyltetrahydro-1,4-thiazine. The molecular and crystal structures of 1-aza-3-oxa-7-thiabicyclo3.4.0]nonan-2-one were investigated by x-ray diffraction analysis.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, pp. 1280–1285, September, 1986. |
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