| 含高碳糖片断的氨基醇及水解产物的波谱分析 |
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| 引用本文： | 邹大鹏,朱卫国,刘宏民.含高碳糖片断的氨基醇及水解产物的波谱分析[J].波谱学杂志,2005,22(3):277-283. |
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| 作者姓名： | 邹大鹏 朱卫国 刘宏民 |
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| 作者单位： | 郑州大学 化学系，河南 郑州 450052 |
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| 摘 要： | 利用C10高碳糖合成了具有潜在生物活性的含有高碳糖结构片断的氨基醇，检测了该氨基醇及其水解产物的1H、13C NMR图谱，确证了该类化合物的结构，通过1H-1H COSY，HMQC，HMBC等2D NMR 技术对其水解产物的1H和13C NMR数据进行了全归属和较详细的解析.
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| 关 键 词： | NMR 归属 2D NMR 高碳糖 氨基醇 |
| 文章编号： | 1000-4556（2005）03-0277-07 |
| 收稿时间： | 2005-04-14 |
| 修稿时间： | 2005-06-09 |
Structure Elucidation of A Higher Carbon Sugar-Derived Amino Alcohol and Its Hydrolysate by NMR |
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| ZOU Da-Peng,ZHU Wei-guo,LIU Hong-min.Structure Elucidation of A Higher Carbon Sugar-Derived Amino Alcohol and Its Hydrolysate by NMR[J].Chinese Journal of Magnetic Resonance,2005,22(3):277-283. |
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| Authors: | ZOU Da-Peng ZHU Wei-guo LIU Hong-min |
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| Institution: | Department of Chemistry，Zhengzhou University ，Zhengzhou 450052，China |
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| Abstract: | An amino alcohol and its hydrolysate, which are potential glycosidase inhibitors, were synthesized from C10 higher carbon sugar. The structures of these novel higher carbon sugar-derived compounds were elucidated by NMR. The ^1H and ^13C chemical shifts of the hydrolysate of the amino alcohol were completely assigned by 2D NMR techniques including ^H-^H COSY, HMQC and HMBC. |
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| Keywords: | NMR 2D NMR |
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