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用于扫描探针显微镜研究的原子级平整金基底的制备
引用本文:江鹏,程广军,张浩力,蔡生民,刘忠范.用于扫描探针显微镜研究的原子级平整金基底的制备[J].物理化学学报,1998,14(7):609-614.
作者姓名:江鹏  程广军  张浩力  蔡生民  刘忠范
作者单位:Center for Intelligent Materials Research(CIMR),College of Chemistry and Molecular Engineering,Peking University,Beijing 100871
基金项目:国家攀登计划,自然科学基金
摘    要:报导了一种用于扫描深外显微镜(SPM)研究的原子级平整全基底的制备方法.采用这种方法,得到了25um2范围内,膜的平均粗糙度小平0.4nm的原子级平整基底,并且得到金以(111)面取向在云母表面沉积的实验证据,同时使用电化学循环伏安法和X光电子能谱对这种膜的自组装性能进行了考察.

关 键 词:扫描探针显微镜(SPM)  金基底  自组装  
收稿时间:1997-11-13
修稿时间:1998-01-16

Preparation of Atomically Flat Stripped-gold Substrate for Self-assembly
Jiang Peng,Cheng Guangjun,Zhang Haoli,Cai Shengmin,Liu Zhongfan.Preparation of Atomically Flat Stripped-gold Substrate for Self-assembly[J].Acta Physico-Chimica Sinica,1998,14(7):609-614.
Authors:Jiang Peng  Cheng Guangjun  Zhang Haoli  Cai Shengmin  Liu Zhongfan
Institution:Center for Intelligent Materials Research(CIMR),College of Chemistry and Molecular Engineering,Peking University,Beijing 100871
Abstract:A method for preparing of atomical flat gold substrate was reported. A series of gold substrates were prepared with the method from 25 C to 270 C and were characterized by using Scanning probe Microscope(SPM). The results show that the mean roughness values of these gold substrates are smaller than 0.4 nm for areas of 25 μm2. A higher resolution image made by using Scanning Tunneling Microscope (STM) shows a hexagonal pattern of high spots with nearest neighbor spacing of 0.30±0.04 nm, which is consistent with a Au-(111) lattice. Meanwhile, self-assembled monolayer film of 1,6-hexanedithiol on the gold has been characterized by electrochemical cyclic voltammetry and X-ray photoelectron spectra.
Keywords:Stripped-gold substrate  Scanning probe microscope  Self-assembly  
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